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DIBAL‐H‐mediated demethylation provides a novel method to access secondary‐rim functionalized γ‐cyclodextrin. 2A,3B‐Dihydroxyl‐per‐O‐methylated‐γ‐cyclodextrin has been obtained, whose conjugation with C60 allows access to the most water‐soluble C60 conjugate described so far. The water solubility of 0.12 m (550 mg mL−1) is 150 times higher than that of the native γ‐CD/C60 complex. Its singlet oxygen (1O2) quantum yield is 0.39, an increase of one to two orders of magnitude compared to that of α(β)CD–C60 conjugates.
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Zhu et al. (2017) studied this question.
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