Solid-state syntheses of acyl thiosemicarbazides are reported for the first time. Eleven acyl thiosemicarbazides have been synthesized at room temperature in excellent yields (84.5 ∼ 91.0%). Among them, eight compounds 3a, 3d, 3e, 3g–k are new. The reaction proves to be extremely simple and highly efficient (in 6 ∼ 18 min).
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Li et al. (2001) studied this question.
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