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The first total synthesis of clavicipitic acid , a derailment product of ergoline biosynthesis, has been accomplished through an intramolecular azide cycloaddition reaction.The 3,4-disubstituted indole required for this work was assembled from indole-4-carboxaldehyde.The single imine generated from the [ 3 + 2 ] cycloaddition reaction was subjected to bromination, dehydrobromination,
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Kozikowski et al. (1982) studied this question.
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