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Regioselective and stereoselective radical additions of arenethiols to various ynamides have been developed.Mixing ynamides and arenethiols in the presence of a catalytic amount of triethylborane affords the corresponding adducts, (Z)-1-amino-2thio-1-alkenes, in excellent yields with high selectivities.The products can be reduced by means of trifluoroacetic acid and triethylsilane to yield 1-amino-2-thioalkanes.
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Yorimitsu et al. (2008) studied this question.
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