This study represents a new technique to synthesize graphenenano sheets, where Graphene Oxide (GO) was synthesized by oxidation of graphite flakes via modified Hummers method. The produced GO was thermally reduced (exfoliated) at 350 C for 1, 3, 6 and 9 hours to produce graphenenano sheets having different degrees of reduction assigned as R1, R3, R6 and R9. The influence of reduction time on the physical properties of graphene was investigated using X-ray Diffraction (XRD) and Thermal Analysis (TGA) to study the phase composition.
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Mm et al. (2017) studied this question.
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