Synthesis and structural characterization using synchrotron radiation of [(C 6 H 13 N 2 ) 2 (H 3 O)(H 2 O)][AgGe 4 S 10 ](dabco–AgGS–SB2): knitting sulfide metal clusters to form frameworks

A novel framework comprised of [Ge4S10]4– adamantine clusters linked by Ag+ is synthesized hydrothermally and its structure determined utilizing data collected on a 36 pl (36 × 10–12 l) single crystal using an X-ray synchrotron/imaging plate combination.