A one-pot approach reveals successful preparation of bis-phosphonates, indicating low-cost methods can achieve radical reaction efficiency.
A one‐pot access to alkyl‐bisphosphonates and alkyl‐bisphosphinates was developed using affordable starting materials (terminal alkynes and low‐cost photoinitiator), no metal catalyst, neither ligand, and no or little amounts of solvents. The radical reaction proceeded smoothly under UV exposure, the reaction conditions were optimized and the scope of the reaction was explored.
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Vasco et al. (2025) studied this question.
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