Facile syntheses of ribonucleoside 5′-triphosphates have been accomplished in good yield (>60%) in a one-pot reaction of unprotected nucleosides with phosphoryl chloride followed by treatment of the resulting phosphorodichloridate with tri-n-butylammonium phosphate in the presence of dimethylformamide.
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Mishra et al. (1991) studied this question.
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