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The construction of a high-temperature diffractometer furnance for quantitative x-ray intensity measurements to above 2000°C is described. The details include descriptions of a new sample holder, the hot-zone geometry and assembly, the radiation shielding, direct temperature measurement and a continuously adjustable specimen rocking device. Emphasis has been placed upon flexibility and reliable high-temperature operation. Although the system is operated with a Siemens diffractometer, it could be used with any diffractometer operating on a horizontal plane.
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Houska et al. (1964) studied this question.
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