By in situ high-pressure i.r. spectroscopy acetyl [MeCO] as a possible intermediate for C2-oxygenates and acetate surface species are observed over Rh/SiO2 and Rh–Mn/SiO2 catalysts in a CO–H2 reaction (CO/H2= 0.5, 30–50 kg/cm2, 230–270 °C).
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Fukushima et al. (1985) studied this question.
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