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The Coprecipitation reaction of Zn2+ and Al3+ ions in moderately acidic α-[SiW11O39]8– solution directly affords a layered double hydroxide derivative with an approximate composition of [Zn24Al8(OH)64][α-SiW1lO39] and an exceptionally well-ordered gallery height of 9.8 Å.
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Narita et al. (1993) studied this question.