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The palladium(II) decorated tungstobismuthate(III) [Pd3 (H2O)9Bi2W22O76]8− (1) has been prepared by a simple one-pot reaction of PdCl2 with Na12[Bi2W22O74(OH)2] in aqueous acidic medium at pH 4.8. Polyanion 1 represents a rare example of a structurally characterized palladium-containing polyoxometalate.
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Bi et al. (2009) studied this question.
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