2,4-Dienes are prepared in high yields with high regioselectivity by the codimerisation of acetylenes and alkenes in the presence of a catalytic amount of Ru(cod)(cot) at 80 °C cod = cycloocta-1,5-diene, cot = cycloocta-1,3,5,-triene.
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Mitsudo et al. (1991) studied this question.
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